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Try this:
1.) On the desktop ActiveSync connection settings, check "Allow serial cable or infrared connection to this COM port". Change the dropdown list to Infrared Port (IR).
2.) Point the IR transmitter/receivers at each other and wait for your desktop to detect the PPC.
3.) On the PPC ActiveSync, tap the Tools menu and select Connect via IR...
This works for my laptop running XP Pro with ActiveSync 3.7.1.
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